UCLA Geocheminar
ESS 235B

Winter 2008 Schedule
Seminars held Wednesdays, 4:00pm-5:00pm in 4660 Geology


Jan. 9: No Seminar - Andrea Ghez Science Colloquium, 1425 Physics

Jan. 16: Jonathan Hunt (UCLA)
Speciation of aqueous silica using Raman spectroscopy and first principles calculations

Abstract:

Dissolved silica plays an important role in lithospheric fluid chemistry. Silica concentrations in quartz-saturated aqueous fluids vary over the range of crustal temperatures and pressures enough to allow for significant mass transport of silica via fluid-rock interaction. The polymerization of silica could afford silicate crystal-like or melt-like sites to otherwise insoluble elements such as titanium, leading to enhanced mobility for those elements. It would therefore be useful to understand what the independent effects of concentration, composition (pH and incorporation of other elements), pressure, and temperature are on silica polymerization. This study presents Raman spectra of high-pH silica solutions taken at ambient conditions with varying silica concentrations. First principles calculations of explicitly solvated silica monomers and dimers are used to interpret the experimental spectra. The results are a promising first step towards a set of experiments to be done in a hydrothermal diamond anvil cell, independently exploring the effects of temperature, pressure, and concentration on silica polymerization.

Jan. 23: Ming-Chang Liu (UCLA)
What can hibonite tell you about early Solar System irradiations?
Abstract:
Energetic particle irradiation by the hyper-active Sun is an important early solar system process. Interactions of energetic projectiles with targets would result in some isotopic effects that might be recorded by early solar system materials. In this talk, I will introduce some astronomical evidence for energetic events and discuss how refractory materials from the early solar system can tell us about these processes.
Jan. 30: Mark Harrison (UCLA)
Diffusion of Ar in muscovite
40Ar/39Ar analysis of muscovite treated at high temperature and water pressure in a piston cylinder apparatus yield a linear array indicative of 40Ar* transport by volume diffusion.  However, the in vacuo 40Ar/39Ar degassing behaviour of the hydrothermally treated material is characterised by both convex and concave forms.  This distinctive age spectra shape differs from that expected from a sample that has been outgassed from a single diffusion domain.  SEM textural characterization of the run products shows that, despite careful pre- and post-hydrothermal experiment sieving of the muscovites, the size population of the run material is not uniform.  We investigated the hypothesis that the form of in vacuo gas release is due to loss of 40Ar* from multiple diffusion domains.  A numerical model constructed to test this hypothesis yields excellent fits between synthetic and actual degassing spectra, supporting the multiple diffusion domain hypothesis.  However, the presence of multiple diffusion domains in the hydrothermal run products impact calculated diffusion parameters.  Deconvolution of the contribution of multiple diffusion domains to the experimentally determined factional loss yield estimates of D that are an order of magnitude lower than that assuming bulk loss of a single domain size.  Diffusion data generated in this manner indicate an activation energy of 64±6 kcal/mol and log Do of 8 cm2/sec and an activation volume for Ar of 2-6 cm3/mol.  These values correspond to a closure temperature (Tc) of 415°C for a muscovite grain with a 100 µm radius cooling at 10°C/Ma at 10 kbar and ca. 390°C at 5 kbars.
Feb. 6: Weifu Guo (Caltech)
Kinetic isotope effects during carbonate clumped isotope fractionation and quantitative speleothem thermometry
Feb. 13: Dianne Taylor (UCLA)
Chronology of large-scale silicate differentiation on the Moon: The Lu-Hf perspective
A timescale for the cooling and crystallization of the lunar magma ocean has not been firmly established, and is essential to the understanding of the silicate differentiation of the terrestrial
planets.  Using the long-lived 176Lu-176Hf isotope system coupled with U-Pb ages of ancient lunar zircons, a closure age for KREEP (representing the last part of the magma ocean to crystallize) has been obtained.  Our results indicate that the large-scale differentiation of the lunar crust was complete by 4.50 Ga.
Feb. 20: Jeremy Boyce (UCLA)
Laser Microprobe (U-Th)/He Thermochronometry
The (U-Th)/He thermochronometer (sensitive to temperatures below 300°C) has been recently applied to a diverse set of Earth science problems including the fields of tectonics, geomorphology, tephrochronology, and meteorite studies.  Unfortunately, (U-Th)/He is a time-consuming technique with poor reproducibility and stringent sample requirements.

I will present an alternative to conventional (U-Th)/He, employing in situ techniques including laser ablation.  Laser microprobe (U-Th)/He can generate ages that are as precise and accurate as conventional (U-Th)/He, but can be applied to crystals that are otherwise not amenable to (U-Th)/He.  This technique also allows tests of reproducibility within single grains, increases throughput, and permits characterization of crystals prior to analysis, further reducing errors.  Applications from 450 Ma to less than 1 Ma will be discussed, as well as the future of laser microprobe (U-Th)/He, which includes micron-scale depth profiling, and direct measurement of key physical parameters essential to (U-Th)/He: diffusivity and alpha-ejection distances.
Feb. 27: Kathryn Dyl (UCLA)
In-Situ UV-Laser Fluorination Oxygen Isotopic Analyses of an Efremovka CAI and Matrix: Implications for Oxygen Isotope Exchange in the Solar Nebula
The oxygen isotope anomaly present in CAIs reveals the earliest evolution of solar system materials. Of specific concern in this study is how the oxygen isotopic composition of various mineral phases in an individual CAI can be related to its thermal and temporal history.  We used the unique UV-laser ablation fluorination technique to obtain high-precision in situ data for E44, a type B CAI from the reduced CV Efremovka.  Using these results, as well as diffusive exchange coefficients for the phases in question, we determined that the oxygen isotopes in anorthite, melilite, and fassiate in E44 could be explained by solid-state oxygen isotopic exchange between this object and a nebular gas.
March 5: Max Coleman (JPL)
Oxygen isotopes to characterize pyrite oxidation processes: latest score in Rio Tinto field versus lab experiments
For more than 20 years there have been publications on characterization of the processes of microbial and inorganic oxidation of pyrite. There has been consensus neither on the mechanism(s) nor on how well oxygen isotopes might quantify the respective contributions from atmosphere and water to oxygen in the sulfate. We have made further lab culture experiments and analyses to add to the confusion but our new results indicate plausible reaction mechanisms. Geochemical data from the Rio Tinto area of Southern Spain have been valuable in identifying different processes in this immense area of acid mine drainage. There are two main end-members in mixtures of very low pH (0.9-1.7), iron sulfate waters: those with Fe(III) and lower �18O values (~4.0‰) and the Fe(II) end-member with more positive �18O (11.2-13.0‰).  We are not convinced that these data quantify the contributions from the oxygen sources but can be used to identify processes occurring in inaccessible parts of the system.
March 12: Haibo Zou (UCLA)
Radiogenic Isotope Constraints on the Origins of Continental Basalts From a Diffuse Igneous Province